科研成果/PUBLICATION

2017
Liu K, Ostadhassan M. Quantification of the microstructures of Bakken shale reservoirs using multi-fractal and lacunarity analysis. Journal of Natural Gas Science and Engineering [Internet]. 2017;39:62-71. 访问链接Abstract
Pore structures are one of the most important factors affecting the hydro-mechanical properties of the reservoirs. Unlike the homogeneous pore structures in sandstones, the pores in the shale formations are heterogeneous and more complex to characterize due to the diagenesis and geological processes that they experienced. The heterogeneous rock pore structures can influence not only the flow properties of the oil and gas but also the fracture initiation and propagation characteristics which can impact the hydraulic fracturing performance, a common technique to increase the total production in tight shale formations. Therefore, quantifying the heterogeneities of the pore structures in unconventional shale formations carries a great importance. In this paper, we collected the samples from Bakken formation, which is a typical unconventional oil shale reservoir in North America. We applied image analysis method to study the pore structures. After segmentation of these images, we determined the representative elementary area (REA) of the samples based on the relationships between porosity and magnification ratios. Multifractal theory and lacunarity methods were applied to analyze the pore structures. Multifractal parameters were used to describe the pore probability distributions and the lacunarity value was applied to quantify the heterogeneity of the pores. The impact of the mineral compositions on heterogeneity values is also discussed. Finally, a new REA indicator, which contains the porosity and heterogeneity information, was proposed.
2016
Liu K, Ostadhassan M, Bubach B. Applications of nano-indentation methods to estimate nanoscale mechanical properties of shale reservoir rocks. Journal of Natural Gas Science and Engineering [Internet]. 2016;35:1310-1319. 访问链接Abstract
In order to study the mechanical properties of shale samples from Bakken Formation, nanoindentation method, an imaging technique borrowed from other engineering disciplines, was used. Different types of nanoindentation curves were analyzed and the applicability of the nanoindentation theories to study mechanical properties of shale samples at nanoscale was demonstrated. Elastic modulus and Hardness of different samples were calculated, compared and related to their mineral compositions and microstructures which are detected by 2D XRD and FESEM methods, respectively. Results showed that samples with more clay minerals (mainly composed of illite) and larger pore structures have less Young's modulus. In addition, based on the energy analysis method, the fracture toughness at nanoscale was estimated and its relationships with Young's modulus was quantified. It was observed that fracture toughness increases linearly with Young's modulus. This paper presents the results and main findings of this study.

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